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71.
A facile and effective method was proposed to prepare the molecularly imprinted fluorescence sensor with carbon quantum dots, which were modified vinyl groups by acrylic acid on the surface. The obtained fluorescence composite material was investigated by transmission electron microscope and Fourier transform infrared spectra. After the experimental conditions were optimized, a linear range of 1.0–60 μmol L−1 was obtained and the detection limit was 0.17 μmol L−1. The novel fluorescence sensor can be successfully used to detect tetracycline in real samples. This study provides a convenient strategy for selective recognition and rapid detection of tetracycline in the complex environment. 相似文献
72.
套管屈服强度直接影响套管抗挤压性能,套管在加工孔过程中可能诱发孔眼附近材料发生金属相变,导致套管屈服强度不再均匀分布,进而影响套管抗挤压强度。在相同工况下,对比了P110完整套管和机加工孔套管的抗挤压强度,以此为参照组分析了相变区域面积和相变区域屈服强度对机加工孔套管抗挤压强度的影响。结果表明,机加工孔会改变材料屈服强度,进而影响套管抗挤压性能。随金属相变区域屈服强度减小,机加工孔套管抗挤压强度减弱;当金属相变区域屈服强度增大时,机加工孔套管抗挤压强度增强。且机加工孔套管相变区域面积对机加工孔套管抗挤压强度的影响随相变区域屈服强度增加而逐渐削弱。 相似文献
73.
针对电站锅炉回转式空气预热器运行时上下表面不可见的问题,本文提出了一种视频监控与故障分析系统,可直接监测转子表面情况。该系统通过视频监控获取图像,结合改进的Retinex算法对其进行处理,实现了以下2个功能:1)能分析积灰程度以判断转子堵塞 情况;2)与温度场融合实时显示转子表面热点分布以预防二次燃烧。该系统已应用于某600 MW机组,实现了在热态环境下对空气预热器转子积灰程度、热点分布、堵塞程度的估算与可视化,大大提高了空气预热器运行的可靠性。 相似文献
74.
Hechun Cao Hui Zheng Lining Fan Zifeng Cheng Jianwei Zhou Qiong Wu Peng Zheng Liang Zheng Yang Zhang 《International Journal of Applied Ceramic Technology》2020,17(2):813-822
In this study, yttrium iron garnet co-doped with Zn and Zr atoms with a chemical formula Y3ZnxZrxFe(5−2x)O12 (x = 0.0-0.3) has been successfully prepared by the solid-state reaction method. The effects of doping concentration on the microstructure, crystal structure, magnetic properties, and dielectric properties of Y3ZnxZrxFe(5−2x)O12 were investigated. The microstructure analysis indicates that co-doping of YIG with Zn and Zr can effectively reduce the grain size of the ceramic. The crystal structure results reveal that the doping concentration of Zn–Zr has substantial influence on the lattice parameters of YIG, such as, increases the lattice constant, crystal cell size, and interplanar spacing. However, the second phase of ZrO2 appears once x ≥ 0.15. Additionally, the dielectric properties of YIG ferrite can be regulated using this Zn–Zr co-doping method. Zn–Zr co-doping can improve the dielectric stability and reduce the dielectric loss at high temperature. The magnetization measurement shows that the saturation magnetization is stabilized at x < 0.15, and the magnetic loss is decreased with the increase in the doping concentration. Overall, the findings show that the ceramic with x = 0.1 exhibits better properties included high saturation magnetization (24.607 emu/g), low magnetic loss (0.0025 @ 1 MHz), and relatively low dielectric loss (496 @ 400°C). 相似文献
75.
Shuncheng Liu Kejian Wang Zhongfeng Zhang Yueqing Ren Lanlan Chen Xiaojie Sun Wenbin Liang 《Polymer Engineering and Science》2020,60(10):2640-2652
Three kinds of ethylene-octene copolymers (POE) were melt-blended with high-density polyethylene (PE-HD) in different proportions. Detailed characterizations were conducted to analyze their structural differences of POE and its effects in toughening PE-HD. The higher molecular weight POE can improve the toughness of PE-HD. 60:40 PE-HD/POE is elongated to break up to 700% while impact strength is 84.7 kJ/m2 at −30°C, which is 21-fold of PE-HD. In the brittle to ductile transition (BDT) during impact, the fracture mechanism changes from the crazing mode to the shear yield-plastic deformation mode. The BDT temperature decreases as the POE molecular weight and its content increase. The interface strength in tension is estimated to access their effects. The Boltzmann-type models were successfully extended to describe the typical S-shaped curves in BDT of notched impact strength vs POE content or temperature. The supplementary decay model is suggested for the attenuation in toughening. Transition map in impact is proposed to select the use range of composition (c ) and temperature (T ) for high toughness. The curves are converted into 3D graph of T -c -impact strength for illustrating their coupling-separate effects, and further into the contour map of impact strength in T -c space for finding their partial equivalence. 相似文献
76.
Wenyun Yang Qiwei Hu Guanyi Qiao Liang Zha Shunquan Liu Jingzhi Han Honglin Du Yan Zhang Yingchang Yang Changsheng Wang 《中国稀土学报(英文版)》2019,37(10):1102-1107
In this work, we report the tuning effect of the Si substitution on the magnetic and high frequency electromagnetic properties of R2Fe17 compounds and their paraffin composites. It is found that the introduction of Si can remarkably improve the magnetic and electromagnetic properties of the R2Fe17 compounds, making the R2Fe17–xSix-paraffin composites excellent microwave absorption materials (MAMs). By introducing the Si element, their saturation magnetizations decrease slightly, while much higher Curie temperatures are obtained. Furthermore, better impedance match is reached due to the decrease of the high-frequency permittivity ε′ by about 40%–50%, which finally enhances the performance of the microwave absorption. The peak frequency (fRL) of the reflection loss (RL) curve moves toward high frequency domain and the qualified bandwidth (QB, RL ≤ ?10 dB) increases remarkably. The maximum QB of 3.3 GHz (12.0–15.3 GHz) is obtained for the Sm1.5Y0.5Fe15Si2-paraffin composite (d = 1.0 mm) and the maximum RL of ?53.6 dB is achieved for Nd2Fe15Si2-paraffin composite (d = 2.2 mm), both surpassing most of the reported MAMs. Additionally, a distinguished dielectric microwave absorption peak is observed, which further increases the QB in these composites. 相似文献
77.
78.
淮钢采用90 t顶底复吹转炉-LF-RH-200 mm×200 mm连铸-连轧工艺流程试生产了2炉Φ60 mm链轨节用钢15B36Cr(/%:0.30~0.37C、0.15~0.30Si、1.20~1.50Mn、≤0.040P、≤0.0505、0.20~0.40Cr、≤0.25Ni、≤0.35Cu、≤0.06Mo、0.0005~0. 0030B)。通过加严影响淬透性化学成分,控制出钢碳≥0.08%,转炉有效挡渣和下渣检测系统控制下渣,LF炉铝粒和电石渣面脱氧,RH最低真空度处理20~30 min,结晶器电磁搅拌、末端电磁搅拌和连铸低过热度保护浇铸等工艺措施,15B36Cr钢的化学成分稳定控制在内控范围内,除了B粗以外,其他类型非金属夹杂物级别全部控制在1.0以内,淬透性控制在较窄的范围内,试制钢种关键技术指标达到客户和预期设计要求。 相似文献
79.
80.
研究了水胶比为0.4,水玻璃模数为1.4及Na2O含量为10%(质量分数)时,单掺偏高岭土与复掺偏高岭土和粉煤灰对碱-矿渣复合胶凝材料的凝结时间和早期力学性能的影响.结果 表明,两种复合方式对碱-矿渣复合胶凝材料均有缓凝作用,但复掺时的缓凝效果更明显.单掺时,碱-矿渣复合胶凝材料的早期抗折、抗压强度和折压比基本不随偏高岭土掺量的变化而变化,但其28 d粘接强度随偏高岭土掺量的增加而增大.复掺时,碱-矿渣复合胶凝材料早期抗压强度随粉煤灰掺量的增加而减小;与单掺时相比,该复合胶凝材料72 h抗折强度和折压比分别提高了40%和64%.除此之外,复掺时该复合胶凝材料28 d粘接强度比单掺时提高了45%,但粉煤灰掺量的影响较小. 相似文献